HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → 4-(Bromomethyl)benzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | 4-Methylbenzophenone | HCID 8652 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 4-(Bromomethyl)benzophenone | HCID 122951 | — |
Reaction Steps
To a solution of 4.0 g (20 mmol) of 4-benzoyltoluene and 3.6 g (20 mmol) of N-bromosuccinimide in 120 ml of carbon tetrachloride was added 0.05 g (0.2 mmol) of benzoyl peroxide. The reaction was refluxed for 17 hours, cooled to room temperature and filtered. The filtrate was evaporated and the crude product was taken on without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326905 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-0b639e4f64e548b3b28c9099506c1821 |
| Source note | uspto-grants-1994_07 |