HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19018239, compound → HCID 19018231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19018239 | HCID 19018239 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 19018231 | HCID 19018231 | 67% |
Reaction Steps
A solution 0.7 g (2.0 mmol) of diethyl 4-[((1methyl)cyclohexyl)methoxy]benzylphosphonate and 10 ml of concentrated hydrochloric acid was refluxed for 24 hours. The reaction was cooled to room temperature, filtered and the solids were washed with water. The solids were recrystallized from EtOAc/cyclohexane to give 0.4 g of the product; m.p. 170°-172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326905 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-c4afa89448764f9bb7d7a4d861f377b1 |
| Source note | uspto-grants-1994_07 |