HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 19018249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19018242 | HCID 19018242 | — |
| Product | HCID 19018249 | HCID 19018249 | — |
Reaction Steps
A solution of 1.5 g (6.2 mmol) of 3-[4-(bromomethyl)phenyl]propionic acid (U.S. Pat. No. 4,032,533) and 1.2 g (9.3 mmol) of oxalyl chloride in 6 ml of dichloromethane was stirred at room temperature for 2.5 hours and evaporated to give 1.6 g of product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326905 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-2f5afa9dd90d48d7938ed920add6dfcd |
| Source note | uspto-grants-1994_07 |