Hydrochloric Acid → HCID 19014332, compound

HRID 1728554Notes

Reaction equation

HRID 1728554 reaction equation
[ClH:1].[CH3:2][C:3]1[N:4]([CH3:20])[C:5](=[N:18][CH3:19])[C:6]2[CH:11]=[CH:10][N:9]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[C:7]=2[N:8]=1>CCCCCC>[ClH:1].[CH3:2][C:3]1[N:4]([CH3:20])[C:5](=[N:18][CH3:19])[C:6]2[CH:11]=[CH:10][N:9]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[C:7]=2[N:8]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19014324HCID 19014324, compound

Product 1

HCID 19014332HCID 19014332, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Hydrogen chloride gas was passed into a solution of 2,3-dimethyl-4-methylimino-7-phenyl-3H,7H-pyrrolo[2,3-d] pyrimidine in hexane to give a precipitate. The precipitate was collected by filtration and dried to afford 2,3-dimethyl-4-methylimino-7-phenyl-3H,7H-pyrrolo[2,3-d] pyrimidine hydrochloride as a solid, mp 257°-258° C.

Workup

  1. customto give a precipitate
  2. filtrationThe precipitate was collected by filtration
  3. customdried

Sources & evidence

ORD record
ord-b385602bca5a4d4fbefaa86aa4ffc2dc
Source dataset
uspto-grants-1994_07
Patent number
US05328910

Reaction notes

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