HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67842554, compound → HCID 19016526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67842554 | HCID 67842554 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 19016526 | HCID 19016526 | 89.7% |
Reaction Steps
The 4-nitrophenylhydrazone of ethyl 2-oxopentanoate (D29) (0.72 g, 2.60 mM) was heated to reflux for 16 h in concentrated hydrochloric acid. After cooling to room temperature the precipitated solid was filtered off. Chromatography on silica using dichloromethane as eluant gave the title compound as a yellow solid (0.22 g; 45%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328922 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-15b103780a3c45b68d45661a388de054 |
| Source note | uspto-grants-1994_07 |