HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-fluoro-2-(trifluoromethyl)- → HCID 131718541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-fluoro-2-(trifluoromethyl)- | HCID 9807 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19014393 | HCID 19014393 | — |
| Reactant | HCID 131718540 | HCID 131718540 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131718541 | HCID 131718541 | — |
Reaction Steps
Preparation as described for compound (11) using 1 g of compound (12), 2-fluorobenzotrifluoride (1.2 g) and NaH (0.174 g) in DMF (100 ml). The crude product was precipitated as the hydrochloride from acetone-ether giving 0.4 g of crystals. M.p. 213.9°-214.9° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328917 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-5949bc5685314dd785be0ce9cafc2cb5 |
| Source note | uspto-grants-1994_07 |