HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloroethyl chloroformate → HCID 131718545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloroethyl chloroformate | HCID 521305 | — |
| Reactant | HCID 131718534 | HCID 131718534 | — |
| Reactant | HCID 131718539 | HCID 131718539 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 131718545 | HCID 131718545 | 62% |
Reaction Steps
Was prepared from compound (13) (3 g) and 1-chloroethyl chloroformate (1 g) in dry 1,2-dichloroethane (50 ml) as described for compound (6 ). Yield 62%. M.p. 195.5°-199.6° C. (d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328917 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-241f5516565e46f7b72745003753b04c |
| Source note | uspto-grants-1994_07 |