HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-[[Acetyl[3-(tetradecyloxy)benzoyl]amino]methyl]-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-Acetyl-N-(2-pyridinylmethyl)-3-(tetradecyloxy)benzamide | HCID 10367289 | — |
| Product | 2-[[Acetyl[3-(tetradecyloxy)benzoyl]amino]methyl]-1-methylpyridinium iodide | HCID 10416273 | 98% |
Reaction Steps
The title compound is prepared by the procedure of Example 28, using 1.08 g of product from Example 29 and 16.36 g of methyl iodide. The residue is recrystallized from methyl alcohol to give 1.38 g of the desired product as yellow crystals with hygroscopic properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-141d72d42250406a9e2bdfcc41767006 |
| Source note | uspto-grants-1994_07 |