huagongshe.com
HRID1728814

反应详情

EQUATION

反应方程式

HRID 1728814 的结构方程式

REACTANTS

反应物

2
结构：CI
HCID6328

Methyl iodide

CH3I

结构：CCCCCCCCCCCCCCOc1cccc(C(=O)N(Cc2ccccn2)C(C)=O)c1
HCID10367289

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCOc1cccc(C(=O)N(Cc2cccc[n+]2C)C(C)=O)c1.[I-]
HCID10416273

未命名化合物

收率 98%

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 28, using 1.08 g of product from Example 29 and 16.36 g of methyl iodide. The residue is recrystallized from methyl alcohol to give 1.38 g of the desired product as yellow crystals with hygroscopic properties.

WORKUP

后处理

  1. customThe title compound is prepared by the procedure of Example 28
  2. customThe residue is recrystallized from methyl alcohol