HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-[[Acetyl[[4-(hexadecyloxy)phenoxy]acetyl]amino]methyl]-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-Acetyl-2-[4-(hexadecyloxy)phenoxy]-N-(2-pyridinylmethyl)acetamide | HCID 19016359 | — |
| Product | 2-[[Acetyl[[4-(hexadecyloxy)phenoxy]acetyl]amino]methyl]-1-methylpyridinium iodide | HCID 19764673 | 88.1% |
Reaction Steps
The title compound is prepared by the procedure of Example 28, using 0.268 g of product from Example 90 and 3.63 g of methyl iodide. The residue is crystallized from hot methyl alcohol/chloroform to give 0.30 g of the desired product as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-d0eead582af848638cd79b092b1f94d6 |
| Source note | uspto-grants-1994_07 |