HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 1-Ethyl-2-[2-[[[4-(hexadecyloxy)phenoxy]acetyl]amino]ethyl]pyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 2-[4-(Hexadecyloxy)phenoxy]-N-[2-(2-pyridinyl)ethyl]acetamide | HCID 19764678 | — |
| Product | 1-Ethyl-2-[2-[[[4-(hexadecyloxy)phenoxy]acetyl]amino]ethyl]pyridinium iodide | HCID 19015939 | 81.4% |
Reaction Steps
The title compound is prepared by the procedure of Example 8, using 0.50 g of product from Example 92, 7.85 g of ethyl iodide and heating the mixture at 110°-120° C. for 26 hours. The residue is recrystallized from methyl alcohol to give 0.535 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-6a092d357ec44627b8e3a4ba1d06c903 |
| Source note | uspto-grants-1994_07 |