Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 10097364 | HCID 10097364 | — |
| Product | HCID 10394507 | HCID 10394507 | 75.3% |
Reaction Steps
A mixture of 1.01 g of product from Example 49 and 15.83 g of ethyl iodide is heated at 105° C. for 23 hours. The reaction is concentrated in vacuo and triturated with diethyl ether to give 1.0 g of the desired product as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05328921 |
|---|
| Source dataset | uspto-grants-1994_07 |
|---|
| ORD ID | ord-6d998697ed45442faa0bdf5274635f7c |
|---|
| Source note | uspto-grants-1994_07 |
|---|
