1-Iodopropane → HCID 19015355, compound

HRID 1728907Notes

Reaction equation

HRID 1728907 reaction equation
[C:1]1([N:7]([CH2:16][C:17]2[CH:22]=[CH:21][C:20]([O:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])=[CH:19][CH:18]=2)[C:8]([C:10]2[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=2)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[I:38][CH2:39][CH2:40][CH3:41]>>[I-:38].[C:1]1([N:7]([CH2:16][C:17]2[CH:18]=[CH:19][C:20]([O:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])=[CH:21][CH:22]=2)[C:8]([C:10]2[CH:11]=[N+:12]([CH2:39][CH2:40][CH3:41])[CH:13]=[CH:14][CH:15]=2)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 336431-IodopropaneHCID 19015330HCID 19015330, compound

Product 1

HCID 19015355HCID 19015355, compoundYield 998.5%

Conditions

Temperature
100 °C

Procedure

A mixture of 0.080 g of product from Example 146 and 13.58 g of iodopropane is heated, in a sealed tube, at 100° C. for 10 hours. The reaction is concentrated in vacuo to give 1.07 g of the desired product as orange crystals.

Workup

  1. concentrationThe reaction is concentrated in vacuo

Sources & evidence

ORD record
ord-49d656bd9ea04463974ca042291e7e05
Source dataset
uspto-grants-1994_07
Patent number
US05328921

Reaction notes

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