HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 52086-51-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21804431 | HCID 21804431 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 52086-51-8 | HCID 19016872 | — |
Reaction Steps
38.45 g (200 mmol) of ester f2, 850 ml of 5% strength NaOH and 850 ml of MeOH were refluxed for 4.5 hours, the MeOH was distilled off, the product was acidified, and the ether extract was dried with MgSO4 and distilled (107°-109° C./high vacuum).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05329033 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-7155b9fd76d04a2fa249fa932102eaf2 |
| Source note | uspto-grants-1994_07 |