HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10997132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 13451547 | HCID 13451547 | — |
| Product | HCID 10997132 | HCID 10997132 | 79.9% |
Reaction Steps
1.18 g of (3S, 4R)-3-methoxycarbonyl-4-methylcyclopentanone was added to 20 ml of 3N-hydrochloric acid, and the mixture was refluxed for 2 hours. The resultant mixture was cooled down to room temperature, and concentrated to dryness. The residue was purified by distillation under a reduced pressure, and thus 0.858 g of the titled compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05329042 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-985eaa37d2ae4d1da45eeea1e0b31458 |
| Source note | uspto-grants-1994_07 |