HuagongsheHuagongshe Chemistry Print Report · For research reference only
Saccharin → HCID 131718560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Saccharin | HCID 5143 | — |
| Reactant | HCID 19013343 | HCID 19013343 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131718560 | HCID 131718560 | 101.6% |
Reaction Steps
In 10 ml of methanol, 0.20 g of 3-(4-tertbutylphenyl)-2,7-dimethyl-1,2,3,4-tetrahydroisoquinoline and 0.13g of saccharin were dissolved at room temperature under stirring, and the resulting mixture was left to stand for 3 hours. The solvent was evaporated under reduced pressure to obtain 0.33 g of 3-(4-tertbutylphenyl)-2,7-dimethyl-l,2,3,4-tetrahydroisoquinoline saccharin salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05330991 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-82eca635883a4d309d05c5973e8fac64 |
| Source note | uspto-grants-1994_07 |