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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1729037Generated: November 1, 2026

Saccharin → HCID 131718560, compound

https://huagongshe.com/reaction/1729037

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSaccharinHCID 5143—
ReactantHCID 19013343HCID 19013343—
SolventMethanolHCID 887—
ProductHCID 131718560HCID 131718560101.6%

Reaction Steps

In 10 ml of methanol, 0.20 g of 3-(4-tertbutylphenyl)-2,7-dimethyl-1,2,3,4-tetrahydroisoquinoline and 0.13g of saccharin were dissolved at room temperature under stirring, and the resulting mixture was left to stand for 3 hours. The solvent was evaporated under reduced pressure to obtain 0.33 g of 3-(4-tertbutylphenyl)-2,7-dimethyl-l,2,3,4-tetrahydroisoquinoline saccharin salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05330991
Source datasetuspto-grants-1994_07
ORD IDord-82eca635883a4d309d05c5973e8fac64
Source noteuspto-grants-1994_07