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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1729038Generated: November 1, 2026

Saccharin → HCID 131718561, compound

https://huagongshe.com/reaction/1729038

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSaccharinHCID 5143—
ReactantHCID 21754773HCID 21754773—
SolventMethanolHCID 887—
ProductHCID 131718561HCID 131718561105.9%

Reaction Steps

In 10 ml of methanol, 0.20 g of 7-tert-butyl-3-(4-tert-butylphenyl)-2-methyl-l,2,3,4-tetrahydroisoquinoline and 0.10 g of saccharin were dissolved under stirring at room temperatureand the resulting mixture was left to stand for 6 hours. The solvent was evaporated under reduced pressure to obtain 0.30 g of 7-tert-butyl-3-(4-tert-butylphenyl)-2-methyl-l,2,3,4-tetrahydroisoquinoline saccharin salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05330991
Source datasetuspto-grants-1994_07
ORD IDord-63b75cbbd6b44226842997cdf00f1609
Source noteuspto-grants-1994_07