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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1729069Generated: November 2, 2026

Ethanol → HCID 54512045, compound

https://huagongshe.com/reaction/1729069

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantSodium CarbonateHCID 10340—
Reactant4-ChlorobenzylamineHCID 66036—
Reactant4-(2-bromoethoxy)-1,2-dichlorobenzeneHCID 280793—
SolventWaterHCID 962—
ProductHCID 54512045HCID 54512045—

Reaction Steps

2.70 Grams (10.0 mmol) of 2-(3,4dichlorophenoxy)ethyl bromide was dissolvedin 30 ml of ethanol, followed by the addition of 1.06 g (10.0 mmol) of anhydrous sodium carbonate and 4.25 g (30.0 mmol) of 4-chlorobenzylamine. The mixture was heated and refluxed on an oil bath for 7 hours. After cooling, the reaction mixture was poured into 100 ml of water and was extracted with chloroform (20 ml×3).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05331011
Source datasetuspto-grants-1994_07
ORD IDord-f6eb65730f824eccbb8798295f631cc8
Source noteuspto-grants-1994_07