HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 54512045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 4-Chlorobenzylamine | HCID 66036 | — |
| Reactant | 4-(2-bromoethoxy)-1,2-dichlorobenzene | HCID 280793 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 54512045 | HCID 54512045 | — |
Reaction Steps
2.70 Grams (10.0 mmol) of 2-(3,4dichlorophenoxy)ethyl bromide was dissolvedin 30 ml of ethanol, followed by the addition of 1.06 g (10.0 mmol) of anhydrous sodium carbonate and 4.25 g (30.0 mmol) of 4-chlorobenzylamine. The mixture was heated and refluxed on an oil bath for 7 hours. After cooling, the reaction mixture was poured into 100 ml of water and was extracted with chloroform (20 ml×3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05331011 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-f6eb65730f824eccbb8798295f631cc8 |
| Source note | uspto-grants-1994_07 |