HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 18653794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 18653795 | HCID 18653795 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18653794 | HCID 18653794 | — |
Reaction Steps
To a stirred solution of N-[(2-adamantyloxy)carbonyl]-β-(2,3-dihydro-1-methyl-5-phenyl-1H-1,4-benzodiazepin-2-yl )-α-methyl-alanine methyl ester (diastereomeric mixture, 5.3 g, 10 mmol) in a mixture of 150 mL dioxane and 75 mL water was added lithium hydroxide (0.72 g, 30 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05331006 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-47d950367dc648b2ade0fa760c6a64b3 |
| Source note | uspto-grants-1994_07 |