HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19012447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19012413 | HCID 19012413 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19012447 | HCID 19012447 | — |
Reaction Steps
A mixture of 404 mg of 6-butyl-1-[4-(2-methoxycarbonylanilinocarbonyl)benzyl]-1,2-dihydro-2-oxopyridine, 10 ml of 0.1N aqueous NaOH solution and 17 ml of THF is left to stand for 48 hours at 20°. The THF is evaporated off, the residue is acidified with HCl and extracted with methylene chloride and the extract is dried over Na2SO4 to give 6-butyl-1-[4-(2-carboxyanilinocarbonyl)benzyl]-1,2-dihydro-2-oxopyridine after evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332750 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-3d7dca667b2f41d8a03f65682e7b9bb0 |
| Source note | uspto-grants-1994_07 |