HRID1729400

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10125141

5-bromo-4-methylpyridine-2,3-diamine

C6H8BrN3

HCID12467710

2-Butyl-1H-imidazo[4,5-b]pyridine

C10H13N3

PRODUCTS

生成物

HCID21464181

6-Bromo-2-butyl-7-methyl-3H-imidazo[4,5-b]pyridine

C11H14BrN3

PROCEDURE

实验过程

The title compound was prepared according to the procedure described for the preparation of 2-butylimidazo[4,5-b]pyridine starting with 5-bromo-2,3-diamino-4-picoline. Yield: 2.54 g (95%) of an amorphous solid: 1H NMR (250 MHz, CDCl3) δ 8.45 (s 1H), 3.05 (t, 2H, J=7 Hz), 2.73 (s, 3H), 2.02-1.87 (m, 2H), 1.61-1.45 (m, 2H), 1.02 (t, 3H, J=7 Hz).