HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86748023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 86748020 | HCID 86748020 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86748023 | HCID 86748023 | — |
Reaction Steps
2-(R)-Hexyl-3-(R)-hydroxy-4-methyl-4-hydroxymethylbutyrolactone (prepared as described in example 7) is reacted with 1 eq. of methanesulfonylchloride and 3 eq. of triethylamine in dry methylene chloride at 0° C. to afford 2-(R)-hexyl-3-(R)-hydroxy-4-methyl-4-methanesulfonyloxymethylbutyrolactone
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332807 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-fb138d0e33ea4c828b9618e2f8ca304a |
| Source note | uspto-grants-1994_07 |