HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethylhydrazine → HCID 73794499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethylhydrazine | HCID 5976 | — |
| Reactant | 1,2-Dimethyl-3-nitrobenzene | HCID 6739 | — |
| Reactant | Hydroxylamine, N-(2,3-xylyl)- | HCID 145678 | — |
| Product | HCID 73794499 | HCID 73794499 | — |
Reaction Steps
Similarly 12.1 g. of 2,3-dimethylnitrobenzene was hydrogenated to 2,3-dimethylphenylhydroxylamine, which was oxidized with ferric chloride to the nitroso compound. This compound was treated with unsymmetrical dimethylhydrazine to yield 3,3-dimethyl-1-(2,3-dimethylphenyl)triazene-1-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989680 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-6d7e241275374f16bad793a338f5c42c |
| Source note | uspto-grants-1976_11 |