HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenyl-3-Buten-2-one → HCID 12391097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenyl-3-Buten-2-one | HCID 15909 | — |
| Reactant | Carbamimidoyl-acetic acid ethyl ester | HCID 4599837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12391097 | HCID 12391097 | 73% |
Reaction Steps
Boiling a solution of 14.6 g of benzylideneacetone and 13.0 g of amidinoacetic acid ethyl ester in 150 ml of ethanol for 2 hours yields 2-amino-6-methyl-4-phenyl-1,4-dihydropyridine-3-carboxylic acid ethyl ester of melting point 150°C (ethanol). Yield: 73 percent of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989708 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-5ee515c516564491a9ed0113e3e4b32a |
| Source note | uspto-grants-1976_11 |