HRID1729688

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID140760

未命名化合物

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

PRODUCTS

产物

反应SMILES：CCOC(=O)C1=C(N)NC(C)=CC1c1ccccc1Cl

HCID193867

Ethyl 2-amino-4-(2-chlorophenyl)-6-methyl-1,4-dihydropyridine-3-carboxylate

C15H17ClN2O2

收率 62%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Upon boiling a solution of 18.1 g of 2-chlorobenzylideneacetone and 13.0 g of amidinoacetic acid ethyl ester in 150 ml of ethanol for 2 hours, 2-amino-6-methyl-4-(2-chlorophenyl)-1,4-dihydropyridine-3-carboxylic acid ethyl ester of melting point 171°C (ethanol) is obtained. Yield: 62 percent of theory.

WORKUP

后处理

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