HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorochalcone → HCID 12391102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorochalcone | HCID 97900 | — |
| Reactant | Carbamimidoyl-acetic acid ethyl ester | HCID 4599837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12391102 | HCID 12391102 | 68% |
Reaction Steps
Upon boiling a solution of 24.3 g of 2-chlorobenzylideneacetophenone and 13.0 g of amidinoacetic acid ethyl ester in 250 ml of ethanol for 3 hours, 2-amino-6-phenyl-4-(2-chlorophenyl)-1,4-dihydropyridine-3-carboxylic acid ethyl ester of melting point 196°C (alcohol) is obtained. Yield: 68 percent of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989708 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-43afe77dfd7f4e93bce9df9677412abe |
| Source note | uspto-grants-1976_11 |