HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanethiol → 2-Pyrazinyl-ethyl methyl sulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Vinylpyrazine | HCID 77840 | — |
| Product | 2-Pyrazinyl-ethyl methyl sulfide | HCID 22630400 | — |
Reaction Steps
h. 2-Pyrazinyl-ethyl methyl sulfide was prepared by reacting vinylpyrazine [c.f. J.Org.Chem. 27, 1363 (1962)] with methylmercaptan by the action of ultra violet light and in the presence of benzoyl peroxide by the method described in Acta Chem. Scand. 8, 295 (1954). The product was identified by mass spectrometry. It has a b.p. of 57°-69° C. at 0.05 mm. Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989713 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-36ad13a4c9b14ca4b07e56790abfbb20 |
| Source note | uspto-grants-1976_11 |