HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 54359873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 178474720 | HCID 178474720 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54359873 | HCID 54359873 | — |
Reaction Steps
The same reaction procedures as Example 1 were carried out by using 2.4 g of 2-[1-(N-ethoxyamino)propylidene]-5,5-dimethylcyclohexane-1,3-dione and 1.75 g of 4-chlorobenzoylchloride, and chloroform was distilled off under reduced pressure and thereby the desired product as a white crystal was obtained after recrystallization the residual material from n-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989737 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-4e48ab3a877c4b018efac6395b91e60b |
| Source note | uspto-grants-1976_11 |