Hydrochloric Acid → HCID 68138108, compound

HRID 1729995Notes

Reaction equation

HRID 1729995 reaction equation
[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][NH:11][CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2.Cl[CH2:16][CH2:17][CH2:18][CH2:19][C:20]([NH2:22])=[O:21].Cl>>[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][N:11]([CH2:16][CH2:17][CH2:18][CH2:19][C:20]([NH2:22])=[O:21])[CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 190471785-ChloropentanamideHCID 214987881,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine

Product 1

HCID 68138108HCID 68138108, compound

Procedure

1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and 5-chlorovaleric acid amide are reacted in accordance with the process described in Example 1. Reaction period 19 hours at 60°. The hydrochloride of the title compound has a M.P. of 194°-196° from ethanol.

Workup

  1. customReaction period 19 hours at 60°

Sources & evidence

ORD record
ord-14abfcc78aaf4330ba9be99f05537801
Source dataset
uspto-grants-1976_11
Patent number
US03991066

Reaction notes

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