Chloroacetamide → HCID 68138060, compound
Reaction equation
[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][NH:11][CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2.Cl[CH2:16][C:17]([NH2:19])=[O:18]>>[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][NH:11][CH:10]3[CH2:16][C:17]([NH2:19])=[O:18])=[CH:7][CH:6]=[CH:5][CH:4]=2Participants
3
Procedure
1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and chloroacetamide are reacted in accordance with the process described in Example 1. Reaction period four hours at 60°. M.P. of the title compound 167°-168° from acetone.
Workup
- customReaction period four hours at 60°
Sources & evidence
- ORD record
- ord-2c7966f1a9e44c80847044c2d851abce
- Source dataset
- uspto-grants-1976_11
- Patent number
- US03991066
Reaction notes
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