HRID1729997

反应详情

EQUATION

反应方程式

HRID 1729997 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 18.5 g of 1,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and 7.1 g of acrylamide in 250 cc of ethanol is boiled at reflux for 6 hours. The reaction mixture is evaporated to dryness, and the resulting title compound is recrystallized from ethanol. M.P. 169°-170°.

WORKUP

后处理

  1. temperatureat reflux for 6 hours
  2. customThe reaction mixture is evaporated to dryness
  3. customthe resulting title compound is recrystallized from ethanol