HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylamide → 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl) propionic acid amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | 1,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine | HCID 21498788 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl) propionic acid amide | HCID 54261802 | — |
Reaction Steps
A mixture of 18.5 g of 1,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and 7.1 g of acrylamide in 250 cc of ethanol is boiled at reflux for 6 hours. The reaction mixture is evaporated to dryness, and the resulting title compound is recrystallized from ethanol. M.P. 169°-170°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03991066 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-728b01fac3b34c7bbc8bf38383c6e929 |
| Source note | uspto-grants-1976_11 |