HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl)-N-methylpropionic acid amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methylacrylamide | HCID 14471 | — |
| Reactant | 1,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine | HCID 21498788 | — |
| Product | 3-(1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridin-2-yl)-N-methylpropionic acid amide | HCID 68138724 | — |
Reaction Steps
1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-C]pyridine and N-methyl acrylamide are reacted in accordance with the process described in Example 6. Reaction period 15 hours. M.P. of the hydrochloride of the title compound 200°-201° from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03991066 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-cd71aac84622406ba4fe7daa84c1092c |
| Source note | uspto-grants-1976_11 |