Hydrochloric Acid → HCID 54490703, compound

HRID 1730003Notes

Reaction equation

HRID 1730003 reaction equation
[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][NH:11][CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2.[C:15]([N:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1)(=[O:18])[CH:16]=[CH2:17].Cl>>[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][N:11]([CH2:17][CH2:16][C:15]([N:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1)=[O:18])[CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 3504731-(piperidin-1-yl)prop-2-en-1-oneHCID 214987881,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine

Product 1

HCID 54490703HCID 54490703, compound

Procedure

1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and acrylic acid piperidide are reacted in accordance with the process described in Example 6. Reaction period nine hours. M.P. of the hydrochloride of the title compound 219°-221° from ethanol (decomp.).

Workup

  1. customReaction period nine hours

Sources & evidence

ORD record
ord-6230112418504fd0b5c7d5dc1daada54
Source dataset
uspto-grants-1976_11
Patent number
US03991066

Reaction notes

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