Ethyl Acrylate → HCID 54360975, compound

HRID 1730006Notes

Reaction equation

HRID 1730006 reaction equation
[CH3:1][C:2]1[C:3]2[C:8]([CH:9]3[C:14]=1[CH2:13][CH2:12][NH:11][CH2:10]3)=[CH:7][CH:6]=[CH:5][CH:4]=2.[CH2:15]([O:17][C:18](=[O:21])[CH:19]=[CH2:20])[CH3:16]>C(O)C>[CH2:15]([O:17][C:18](=[O:21])[CH2:19][CH2:20][N:11]1[CH2:12][CH2:13][C:14]2=[C:2]([CH3:1])[C:3]3[C:8]([CH:9]2[CH2:10]1)=[CH:7][CH:6]=[CH:5][CH:4]=3)[C:16]1[CH:4]=[CH:3][CH:2]=[CH:14][CH:13]=1

Participants

4

Reactant 2

HCID 8821Ethyl AcrylateHCID 214987881,3,4,9b-tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine

Product 1

HCID 54360975HCID 54360975, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 12.5 g of 1,3,4,9b-Tetrahydro-5-methyl-2H-indeno[1,2-c]pyridine and 10 g acrylic acid ethyl ester are heated in 100 ml of ethanol for 3 hours at 80° C and then evaporated to dryness. The title compound is obtained as a colourless oil after distillation under a vacuum of 0.1 Torr.

Workup

  1. customevaporated to dryness

Sources & evidence

ORD record
ord-066fe956f95c416ea754e34cfa59eb24
Source dataset
uspto-grants-1976_11
Patent number
US03991066

Reaction notes

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