Chlorosuccinimide → HCID 21498878, compound

HRID 1730051Notes

Reaction equation

HRID 1730051 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([N:16]2[CH:20]=[N:19][N:18]=[C:17]2[CH2:21][N:22]2[C:26](=[O:27])[C:25]3=[CH:28][CH:29]=[CH:30][CH:31]=[C:24]3[C:23]2=[O:32])=[C:6]([CH:15]=1)[C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)=[O:8].[Cl:33]N1C(=O)CCC1=O>C1C=CC=CC=1>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([N:16]2[C:17]([CH2:21][N:22]3[C:26](=[O:27])[C:25]4=[CH:28][CH:29]=[CH:30][CH:31]=[C:24]4[C:23]3=[O:32])=[N:18][N:19]=[C:20]2[Cl:33])=[C:6]([CH:15]=1)[C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)=[O:8]

Participants

4

Reactant 2

HCID 31398ChlorosuccinimideHCID 21498871HCID 21498871, compound

Product 1

HCID 21498878HCID 21498878, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

5-Bromo-2-[3-(phthalimidomethyl)-4H-1,2,4-triazol-4-yl]-benzophenone (0.01 mole) and N-chlorosuccinimide (0.013 mole) in benzene is stirred and refluxed under a nitrogen atmosphere for 7 hours to give 5-bromo-2-[3-chloro-5-(phthalimidomethyl)-4H-1,2,4-triazol-4-yl]benzophenone.

Workup

  1. temperaturerefluxed under a nitrogen atmosphere for 7 hours

Sources & evidence

ORD record
ord-16a0bd5374f04cd2918dfff1edd84edc
Source dataset
uspto-grants-1976_11
Patent number
US03991070

Reaction notes

Loading…