Phosphorus pentachloride → HCID 12329419, compound

HRID 1730105Notes

Reaction equation

HRID 1730105 reaction equation
[C:1]([C:4]1[CH:17]=[CH:16][CH:15]=[CH:14][C:5]=1[C:6]([O:8][O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:7])(O)=[O:2].P(Cl)(Cl)(Cl)(Cl)[Cl:19]>C1C=CC=CC=1>[Cl:19][C:1]([C:4]1[CH:17]=[CH:16][CH:15]=[CH:14][C:5]=1[C:6]([O:8][O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:7])=[O:2]

Participants

4

Reactant 2

HCID 24819Phosphorus pentachlorideHCID 847692-[(tert-Butylperoxy)carbonyl]benzoic acid

Product 1

HCID 12329419HCID 12329419, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

To a suspension of t-butyl o-(carboxy)peroxybenzoate (16.2g. 0.06 moles) in 100 ml. of benzene at +6° to +24° C but preferably at +6° to +10° C was added in a single portion phosphorous pentachloride (12.6g. 0.06 moles).

Sources & evidence

ORD record
ord-84635f1a780f459496b1ad31ba408a1d
Source dataset
uspto-grants-1976_11
Patent number
US03991109

Reaction notes

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