HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 12329419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2-[(Tert-butylperoxy)carbonyl]benzoic acid | HCID 84769 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12329419 | HCID 12329419 | — |
Reaction Steps
To a suspension of t-butyl o-(carboxy)peroxybenzoate (16.2g. 0.06 moles) in 100 ml. of benzene at +6° to +24° C but preferably at +6° to +10° C was added in a single portion phosphorous pentachloride (12.6g. 0.06 moles).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03991109 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-84635f1a780f459496b1ad31ba408a1d |
| Source note | uspto-grants-1976_11 |