HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → Diallylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Ammonium Persulfate | HCID 62648 | — |
| Reactant | Diallylamine hydrochloride | HCID 521977 | — |
| Reactant | N-Methyl-N-(prop-2-en-1-yl)prop-2-en-1-amine--hydrogen chloride (1/1) | HCID 71354557 | — |
| Solvent | Water | HCID 962 | — |
| Product | Diallylamine | HCID 31279 | — |
| Product | Diallylmethylamine | HCID 75501 | — |
Reaction Steps
Part 1 A copolymer of N-methyl diallylamine and diallylamine is prepared according to the procedure of Example 1, Part 1, except that a mixture of 200 grams of N-methyl diallylamine hydrochloride and 50 grams of diallylamine hydrochloride is substituted for the 258 grams of diallylamine hydrochloride and 455 grams of dimethyl sulfoxide and 5 grams of ammonium persulfate are used. The copolymer (75 grams) is water-soluble, has an RSV of 0.2 and contains by NMR analysis 90 weight percent of N-methyl diallylamine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992345 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-0d9abe7c18a644f59f070b85630f8ca4 |
| Source note | uspto-grants-1976_11 |