Triethylamine → HCID 70604619, compound

HRID 1730315Notes

Reaction equation

HRID 1730315 reaction equation
C(N(CC)CC)C.Cl.[NH2:9][CH:10]1[C:20](=[O:21])[N:12]2[CH:13]([C:18]#[N:19])[C:14]([CH3:17])([CH3:16])[S:15][C@H:11]12>C(Cl)Cl>[NH2:9][CH:10]1[C:20](=[O:21])[N:12]2[CH:13]([C:18]#[N:19])[C:14]([CH3:16])([CH3:17])[S:15][C@H:11]12

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 70604618HCID 70604618, compound

Product 1

HCID 70604619HCID 70604619, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Triethylamine (666 mg., 6.6 mmoles) is added to a suspension of 6-amino-2,2-dimethyl-3-cyanopenam hydrochloride (1.3 g., 6.0 mmoles) in methylene chloride (100 ml.) and the mixture stirred at room temperature for 20 minutes.

Sources & evidence

ORD record
ord-1c45488123b24d3da2be2c5097033ed4
Source dataset
uspto-grants-1976_11
Patent number
US03992394

Reaction notes

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