HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21497739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 3,5-Di-tert-butyl-4-hydroxybenzoyl chloride | HCID 3787187 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21497739 | HCID 21497739 | — |
Reaction Steps
Three moles 3,5-di-t-butyl-4-hydroxybenzoyl chloride and 1 mole diethanolamine in benzene are stirred at room temperature for 16 hours. The reaction mixture is poured into water, the benzene layer is separated and the benzene evaporated under reduced pressure to provide N,N-bis(3',5'-di-tert.-butyl-4'-hydroxybenzoyloxyethyl)-3,5-di-tert.butyl-4-hydroxybenzamide as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992434 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-26ae37853aba4088999af405941be6b4 |
| Source note | uspto-grants-1976_11 |