Water → HCID 21497739, compound

HRID 1730378Notes

Reaction equation

HRID 1730378 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[C:12]([C:15]([CH3:18])([CH3:17])[CH3:16])[C:13]=1[OH:14])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[NH:19]([CH2:23][CH2:24][OH:25])[CH2:20][CH2:21][OH:22].[OH2:26]>C1C=CC=CC=1>[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[C:12]([C:15]([CH3:18])([CH3:17])[CH3:16])[C:13]=1[OH:14])[C:8]([O:22][CH2:21][CH2:20][N:19]([CH2:23][CH2:24][O:25][C:8](=[O:9])[C:7]1[CH:6]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[C:13]([OH:14])=[C:12]([C:15]([CH3:18])([CH3:17])[CH3:16])[CH:11]=1)[C:8](=[O:9])[C:7]1[CH:11]=[C:12]([C:15]([CH3:16])([CH3:17])[CH3:18])[C:13]([OH:26])=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:6]=1)=[O:9])([CH3:4])([CH3:3])[CH3:2]

Participants

5

Reactant 3

HCID 962WaterHCID 8113DiethanolamineHCID 37871873,5-Di-tert-butyl-4-hydroxybenzoyl chloride

Product 1

HCID 21497739HCID 21497739, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Three moles 3,5-di-t-butyl-4-hydroxybenzoyl chloride and 1 mole diethanolamine in benzene are stirred at room temperature for 16 hours. The reaction mixture is poured into water, the benzene layer is separated and the benzene evaporated under reduced pressure to provide N,N-bis(3',5'-di-tert.-butyl-4'-hydroxybenzoyloxyethyl)-3,5-di-tert.butyl-4-hydroxybenzamide as a white solid.

Workup

  1. customthe benzene layer is separated
  2. customthe benzene evaporated under reduced pressure

Sources & evidence

ORD record
ord-26ae37853aba4088999af405941be6b4
Source dataset
uspto-grants-1976_11
Patent number
US03992434

Reaction notes

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