HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → gamma-Aminopropylhydroquinone.hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3-(2,5-Dimethoxyphenyl)propan-1-amine | HCID 21497980 | — |
| Product | gamma-Aminopropylhydroquinone.hydrobromide | HCID 21390156 | 69.3% |
Reaction Steps
100 g of γ-aminopropyl-2,5-dimethoxybenzene was heated at an oil bathtemperature of 180° C in 830 ml of 48% hydrobromic acid while blowing therein nitrogen gas. After the reaction, the reaction mixture wascooled, and the precipitated crystals were filtered out and dried to obtain88 g of the end product having a melting point of 130° ~ 131° C (yield 69.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992449 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-591c58fa673343aca1b1691cce4eb241 |
| Source note | uspto-grants-1976_11 |