HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2-Methoxycyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Chlorocyclohexanone | HCID 13203 | — |
| Product | 2-Methoxycyclohexanone | HCID 110998 | 90% |
Reaction Steps
2-methoxycyclohexanone was prepared as in Example 4, by dissolving 98 gm. 2-chlorocyclohexanone in 750 ml. methanol and heating the solution in a sealed vessel at 160° C. for 15 minutes. The conversion was 98-99% with a yield of greater than 90%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992452 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-4b3b9878e5cc43d99bf558b80deae5ff |
| Source note | uspto-grants-1976_11 |