HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Chloride → HCID 178504058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Chloride | HCID 6327 | — |
| Reactant | 4-Chlorobenzaldehyde thiosemicarbazone | HCID 668099 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178504058 | HCID 178504058 | — |
Reaction Steps
A 10% molar excess of methyl chloride is added to 2.14 g. of 4-chlorobenzaldehyde thiosemicarbazone and 25 ml. of a anhydrous ethanol in a pressure vessel. The reaction mixture is magnetically stirred and heated in an oil bath for 11/2 hour. The crystalline title compound separates on cooling and is filtered off and air dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992446 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-c087c0ad21d346b882b5b33bc6cd4816 |
| Source note | uspto-grants-1976_11 |