Methyl Chloride → HCID 178504058, compound

HRID 1730475Notes

Reaction equation

HRID 1730475 reaction equation
[CH3:1]Cl.[Cl:3][C:4]1[CH:15]=[CH:14][C:7]([CH:8]=[N:9][NH:10][C:11]([NH2:13])=[S:12])=[CH:6][CH:5]=1>C(O)C>[ClH:3].[Cl:3][C:4]1[CH:15]=[CH:14][C:7]([CH:8]=[N:9][NH:10][C:11](=[NH:13])[S:12][CH3:1])=[CH:6][CH:5]=1

Participants

4

Reactant 2

HCID 6327Methyl ChlorideHCID 6680994-Chlorobenzaldehyde thiosemicarbazone

Product 1

HCID 178504058HCID 178504058, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 10% molar excess of methyl chloride is added to 2.14 g. of 4-chlorobenzaldehyde thiosemicarbazone and 25 ml. of a anhydrous ethanol in a pressure vessel. The reaction mixture is magnetically stirred and heated in an oil bath for 11/2 hour. The crystalline title compound separates on cooling and is filtered off and air dried.

Workup

  1. temperatureheated in an oil bath for 11/2 hour

Sources & evidence

ORD record
ord-c087c0ad21d346b882b5b33bc6cd4816
Source dataset
uspto-grants-1976_11
Patent number
US03992446

Reaction notes

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