HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178521124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178524726 | HCID 178524726 | — |
| Product | HCID 178521124 | HCID 178521124 | — |
Reaction Steps
A mixture of 0.5 g of 4-hydroxy-8-trifluoromethyl-3 -quinoline-carboxylic acid in 5 ml of thionyl chloride was stirred at room temperature for 24 hours and the precipitate formed was recovered by vacuum filtration to obtain 0.4 g of 4-hydroxy-8-trifluoromethyl-3-quinoline-carboxylic acid chloride melting at 222° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992540 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-9c960e990a0e4356ac17dfad6c20d1d2 |
| Source note | uspto-grants-1976_11 |