HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hydrazinoisoquinoline → 3-Acetoxymethyl-s-triazolo-[3,4-a]-isoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hydrazinoisoquinoline | HCID 11557333 | — |
| Reactant | Acetoxyglycolic acid | HCID 22133411 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-Acetoxymethyl-s-triazolo-[3,4-a]-isoquinoline | HCID 21498218 | — |
Reaction Steps
1-Hydrazinoisoquinoline was heated with excess acetoxyglycolic acid. The residue was cooled, dissolved in chloroform and washed with sodium carbonate solution. The chloroform extracts were dried and concentrated invacuo to provide the crude product which was purified by recrystallization from benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992539 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-ec8c70329bf748aa9232107ce1873fb3 |
| Source note | uspto-grants-1976_11 |