HRID1730546

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID238012

4-Amino-6-chloropyrimidine

C4H4ClN3

结构：COC(=O)C1=C(O)c2ccc3ccccc3c2S(=O)(=O)N1C

HCID54690651

未命名化合物

PRODUCTS

生成物

结构：CN1C(C(=O)Nc2cc(Cl)ncn2)=C(O)c2ccc3ccccc3c2S1(=O)=O

HCID54695919

未命名化合物

收率 47%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

N-(6-Chloro-4-pyrimidinyl)-4-hydroxy-2-methyl-2H-naphtho[2,1-e]-1,2-thiazine-3-carboxamide-1,1-dioxide was prepared analogous to Example 1 from 4-hydroxy-2-methyl-2H-naphtho[2,1-e]-1,2-thiazine-3-carboxylic acid methylester-1,1-dioxide and 4-amino-6-chloro-pyrimidine. Yield: 47% of theory; m.p. 263° C (decomp.; from xylene).