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HRID1730550

反应详情

EQUATION

反应方程式

HRID 1730550 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc(N)sc1C
HCID73238

4,5-Dimethyl-1,3-thiazol-2-amine

C5H8N2S

结构：COC(=O)C1=C(O)c2ccc3ccccc3c2S(=O)(=O)N1C
HCID54690651

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nc(NC(=O)C2=C(O)c3ccc4ccccc4c3S(=O)(=O)N2C)sc1C
HCID54695946

未命名化合物

收率 31%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCCl
溶剂HCID11

1,2-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

N-(4,5-Dimethyl-2-thiazolyl)-4-hydroxy-2-methyl-2 H-naphtho[2,1-e]-1,2-thiazine-3-carboxamide-1,1-dioxide was prepared analogous to Example 22 from 4-hydroxy-2-methyl-2H-naphtho[2,1-e]-1,2-thiazine-3-carboxylic acid methylester-1,1-dioxide and 2-amino-4,5-dimethyl-thiazole. Yield: 31% of theory; m.p. 264°-265° C (decomp.; from ethylene chloride).